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Reference Electrodes That Use the Same Solvent as the Solution Under Study Silver-Silver Ion Electrode This is the most popular reference electrode used in non-aqueous solutions Since Pleskov employed it in acetonitrile (AN) in 1948, it has been used in a variety of solvents It has a structure as shown in Fig 61(a) and is easy to construct Its potential is usually reproducible within 5 mV, if it is prepared freshly using pure solvent and electrolyte The stability of the potential, however, is not always good enough The potential is stable in AN, because Ag+ is strongly solvated in it In propylene carbonate (PC) and nitromethane (NM), however, Ag+ is solvated only weakly and the potential is easily influenced by the presence of trace water and other impurities.

1) In dimethylformamide (DMF), on the other hand, Ag+ is slowly reduced to Ag0, causing a gradual potential shift to the negative direction 2) This shift can reach several tens of millivolts after a few days Silver-Silver Cryptate Electrode This type of electrode was developed by the present author in order to improve the stability of the silver-silver ion electrode [5] It has a structure of Ag/5 mM AgCrypClO4, 5 mM Cryp, 50 mM Et4NClO4(s), where Cryp and AgCryp+ denote cryptand(22) and its complex with Ag+, respectively, and can be prepared in various solvents Its potential is given by E = E0(Ag+/Ag) 0059 logK+0059 log([AgCryp+]/[Cryp]) (K: formation constant of AgCryp+) Because the electrolyte solution is an Ag+-ion buffer, the potential is stable if the ratio [AgCryp+]/[Cryp] is kept constant Thus, the potential is less influenced by solvent impurities than in the case of an Ag+/Ag electrode.

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Moreover, as in Table 43, the potential of this electrode is not so much influenced by solvent Recently, Lewandowski et al used cryptand(222) to develop a similar reference electrode [6]..

+ P (R|D, S c ) = E |D,S c [E00 (0)] = 0.7143.

These are the basics: ERISA defines a fiduciary as any person so named in the plan and any person who exercises any discretionary authority or control with respect to the management or administration of the plan or its assets With respect to a 401(k) or other qualified retirement plan, the following will normally be included: the plan sponsor, plan administrator, trustees, investment managers, and any other persons, including employees, who are involved with any aspect of handling the plan or its assets Key point: If you are named as a trustee, helped choose the 401(k) provider, participated in the investment selection process, or had a part in making decisions about qualified plan operations, you are a fiduciary A fiduciary s basic duty is to act solely in the interest of the plan s participants and beneficiaries, and for the exclusive purpose of providing benefits to participants and beneficiaries.

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With respect to qualified plan assets, a fiduciary must act prudently, diversify the investments of the plan s assets, and act in a manner consistent with the plan s documents A fiduciary must also act with the care, skill, and diligence under the circumstances that a prudent person, acting in a like capacity and familiar with such matters, would use Fiduciaries must respond fully and accurately to all inquiries from a participant or beneficiary Misleading communications, misrepresentations, or omissions may well constitute a breach of fiduciary duty In selecting a service provider, fiduciaries must consider the quality of the service provided, not merely the costs thereof Plan service providers should be reevaluated periodically.

Fiduciary liability exposure may result from the number of investment choices offered in a 401(k) plan, plan administration expenses, the investment selection process (or lack thereof), long-term investment returns of the plan, and merger and acquisition decisions (reflecting which plans are retained, disposition of investment funds, and so on) Fiduciaries should carefully document their processes with respect to decisions on all aspects of their plan offering and its administration, particularly with respect to the items listed above You should retain: the plan s investment policy statement; investment fund selection due diligence; service provider selection due diligence; ongoing investment monitoring reports; notes of investment committee meetings; plan documents, amendments, and board resolutions; discrimination test results, signed Form 5500s and all compliance documentation; memos distributed to employees concerning your qualified plan; and fidelity bonds.

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